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ChemicalBook CAS DataBase List 1,1,4-Triacetoxy-2,2-dichlorobutane, 98%

1,1,4-Triacetoxy-2,2-dichlorobutane, 98% synthesis

1synthesis methods
141942-52-1 Synthesis
2-ACETOXY-3,3-DICHLOROTETRAHYDROFURAN

141942-52-1
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Butanal, 4-(acetyloxy)-2,2-dichloro-

141942-57-6
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1,1,4-Triacetoxy-2,2-dichlorobutane, 98%

141942-59-8
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Yield:141942-57-6 2% ,141942-59-8 92%

Reaction Conditions:

with sulfuric acid;acetic anhydride at 135; for 48 h;

References:

Buyck, Laurent de;Vanhulle, Peter [Bulletin des Societes Chimiques Belges,1992,vol. 101,# 4,p. 329 - 336]