1,2:5,6-DI-O-CYCLOHEXYLIDENE-MYO-INOSITOL synthesis

2synthesis methods

Product Name:1,2:5,6-DI-O-CYCLOHEXYLIDENE-MYO-INOSITOL
CAS Number:33021-17-9
Molecular formula:C18H28O6
Molecular Weight:340.41

D-myo-Inositol, 2,3:4,5-di-O-cyclohexylidene-

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1,2:5,6-DI-O-CYCLOHEXYLIDENE-MYO-INOSITOL

33021-17-9
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Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: di(n-butyl)tin oxide / toluene / 3 h / Reflux
1.2: 12 h / -40 - 20 °C
2.1: porcine pancreatic lipase / hexane; diethyl ether / 168 h / 37 °C / pH ~ 7 / Aqueous phosphate buffer

References:

US8178704,2012,B2

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33021-17-9
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References

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