1-(4-Methoxybenzylidene)-2-benzylidenehydrazine synthesis

12synthesis methods

Product Name:1-(4-Methoxybenzylidene)-2-benzylidenehydrazine
CAS Number:1149-69-5
Molecular formula:C15H14N2O
Molecular Weight:238.28

4334-74-1 Synthesis

[2-(4-Methoxybenzylidene)hydrazono](amino)methanethiol

4334-74-1
6 suppliers
inquiry

100-52-7 Synthesis

100-52-7
947 suppliers
$20.37/250g

1-(4-Methoxybenzylidene)-2-benzylidenehydrazine

1149-69-5
2 suppliers
inquiry

Yield:-

Reaction Conditions:

with triethylamine in N,N-dimethyl-formamide at 120;Temperature;

Steps:

4.2.1. One-pot synthesis of azines 3a-c

General procedure: A mixture of thiosemicarbazide (5, 0.91 g, 10 mmol) and an aldehyde 6a-c (1 mmol) in DMF (20 mL) containing 10 drops of acetic acid was gently heated at 60°C for 0.5-1 h; thereaction was followed by the TLC analysis. To the reaction mixture, another 10 mmol ofbenzaldehyde (6a) was added and the mixture was heated at 100°C for 15-20 h. After cool-ing, the precipitates 3a-c were allowed to stand overnight, collected by suction filtration,washed with petroleum ether, and dried at room temperature.

References:

Aly, Ashraf A.;Hassan, Alaa A.;Brown, Alan B.;Ibrahim, Mahmoud A. A.;Abdal-Latif, El-Shimaa S. M. [Journal of Sulfur Chemistry,2017,vol. 38,# 1,p. 11 - 17]

3132-92-1 Synthesis