1'-(Aminocarbonyl)-1,2,3,4,5-pentaphenyl-ferrocene synthesis

1synthesis methods

Product Name:1'-(Aminocarbonyl)-1,2,3,4,5-pentaphenyl-ferrocene
CAS Number:894777-14-1
Molecular formula:C35H25.C6H6NO.Fe
Molecular Weight:609.547

Ferrocene, 1'-carboxy-1,2,3,4,5-pentaphenyl-

323187-44-6
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7664-41-7
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1'-(Aminocarbonyl)-1,2,3,4,5-pentaphenyl-ferrocene

894777-14-1
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$684.23/250MG

Yield:894777-14-1 99%

Reaction Conditions:

with oxalyl dichloride;N,N-dimethyl-formamide in methanol;dichloromethane;Fe complex was treated with chloride in CH2Cl2 in presence of DMF (catalyst), then NH3 in methanol at -78°C to room temp.;

References:

Peters, Rene;Xin, Zhuo-Qun;Fischer, Daniel F.;Schweizer, W. Bernd [Organometallics,2006,vol. 25,# 12,p. 2917 - 2920]