1-NAPHTHYLMETHYLPHOSPHONIC ACID synthesis
- Product Name:1-NAPHTHYLMETHYLPHOSPHONIC ACID
- CAS Number:4730-77-2
- Molecular formula:C11H11O3P
- Molecular Weight:222.18
4780-79-4
239 suppliers
$6.00/5g
4730-77-2
20 suppliers
$172.00/500mg
Yield:4730-77-2 75%
Reaction Conditions:
Stage #1: 1-naphthalene methanolwith tris-(dibenzylideneacetone)dipalladium(0);hypophosphorous acid;4,5-bis(diphenylphosphino)-9,9-dimethylxanthene in N,N-dimethyl-formamide at 110; for 15 h;Inert atmosphere;
Stage #2: in N,N-dimethyl-formamide at 110; for 8 h;
References:
Coudray, Laetitia;Montchamp, Jean-Luc [European Journal of Organic Chemistry,2008,# 24,p. 4101 - 4103] Location in patent:supporting information; experimental part
53575-08-9
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$14.00/250mg
4730-77-2
20 suppliers
$172.00/500mg
86-52-2
334 suppliers
$9.00/10g
4730-77-2
20 suppliers
$172.00/500mg