ChemicalBook CAS DataBase List 5-[3,5-DIMETHOXY-4-(FMOC-AMINOMETHYL)PHENOXY]PENTANOIC ACID

5-[3,5-DIMETHOXY-4-(FMOC-AMINOMETHYL)PHENOXY]PENTANOIC ACID synthesis

9synthesis methods

Product Name:5-[3,5-DIMETHOXY-4-(FMOC-AMINOMETHYL)PHENOXY]PENTANOIC ACID
CAS Number:115109-65-4
Molecular formula:C29H31NO7
Molecular Weight:505.56

19009-24-6
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5-[3,5-DIMETHOXY-4-(FMOC-AMINOMETHYL)PHENOXY]PENTANOIC ACID

115109-65-4
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$110.00/1g

Yield:-

Steps:

Multi-step reaction with 5 steps
1: 1.) KOtBu / 1.) DMF, 25 deg C, 2.) 110 deg C, 5h
2: 4N aq. NaOH / methanol / 1 h / 25 °C
3: 95 percent / NH₂OH, Na₂CO₃ / H₂O / 2 h
4: 96 percent / H₂ / 10percent Pd/C / aq. acetic acid / 2 h / 25 °C / 2280 Torr
5: aq. Na₂CO₃ / dioxane / 3 h / 25 °C

References:

Albericio;Kneib-Cordonier;Biancalana;Gera;Masada;Hudson;Barany [Journal of Organic Chemistry,1990,vol. 55,# 12,p. 3730 - 3743]