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(4S,4'S)-2,2'-(Cyclopentane-1,1-diyl)-bis(4-isopropyl-4,5-dihydrooxazole)
(4S,4'S)-2,2'-(Cyclopentane-1,1-diyl)-bis(4-isopropyl-4,5-dihydrooxazole) synthesis
1synthesis methods
- Product Name:(4S,4'S)-2,2'-(Cyclopentane-1,1-diyl)-bis(4-isopropyl-4,5-dihydrooxazole)
- CAS Number:1379452-52-4
- Molecular formula:C17H28N2O2
- Molecular Weight:292.42
Yield: 91%
Reaction Conditions:
Stage #1:1,1-cyclopentanedicarbonitrile with zinc trifluoromethanesulfonate in toluene for 0.166667 h;Inert atmosphere;
Stage #2:(S)-valinol in toluene for 48 h;Inert atmosphere;Reflux;
References:
Choi, Junwon;Fu, Gregory C. [Journal of the American Chemical Society,2012,vol. 134,# 22,p. 9102 - 9105] Location in patent:supporting information; experimental part