1-CHLOROMETHYL-4-FLUORO-1,4-DIAZONIABICYCLO[2.2.2]OCTANE BIS(TRIFLUOROMETHANESULFONATE) synthesis

2synthesis methods

Product Name:1-CHLOROMETHYL-4-FLUORO-1,4-DIAZONIABICYCLO[2.2.2]OCTANE BIS(TRIFLUOROMETHANESULFONATE)
CAS Number:140681-68-1
Molecular formula:C8H14ClF4N2O3S+
Molecular Weight:329.71

33454-82-9 Synthesis

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4-Aza-1-azoniabicyclo[2.2.2]octane, 1-(chloromethyl)-, 1,1,1-trifluoromethanesulfonate (1:1)

141922-62-5
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1-CHLOROMETHYL-4-FLUORO-1,4-DIAZONIABICYCLO[2.2.2]OCTANE BIS(TRIFLUOROMETHANESULFONATE)

140681-68-1
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Yield:140681-68-1 49%

Reaction Conditions:

with fluorine in acetonitrile at -10 - 20;Inert atmosphere;

References:

Teare, Harriet;Robins, Edward G.;Kirjavainen, Anna;Forsback, Sarita;Sandford, Graham;Solin, Olof;Luthra, Sajinder K.;Gouverneur, Veronique [Angewandte Chemie - International Edition,2010,vol. 49,# 38,p. 6821 - 6824] Location in patent:supporting information; experimental part

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140681-68-1
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References

1-CHLOROMETHYL-4-FLUORO-1,4-DIAZONIABICYCLO[2.2.2]OCTANE BIS(TRIFLUOROMETHANESULFONATE) Related Search:

Triethylenediamine N,N-DIETHYLAMMONIUM TRIFLUOROMETHANESULFONATE