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2-(2-chloroethyl)isoindolin-1-one synthesis

3synthesis methods
6270-06-0 Synthesis
N-(2-CHLOROETHYL)PHTHALIMIDE

6270-06-0
54 suppliers
$36.25/1g

2-(2-chloroethyl)isoindolin-1-one

41575-23-9
7 suppliers
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Yield:41575-23-9 92%

Reaction Conditions:

with ethanol;tetrabutylammonium tetrafluoroborate;diisopropylamine at 20; for 2.5 h;Electrochemical reaction;Schlenk technique;Green chemistry;chemoselective reaction;

References:

Bai, Ya;Shi, Lingling;Zheng, Lianyou;Ning, Shulin;Che, Xin;Zhang, Zhuoqi;Xiang, Jinbao [Organic Letters,2021,vol. 23,# 6,p. 2298 - 2302] Location in patent:supporting information