2,2-dimethoxyethylsulfanylmethylbenzene synthesis
3synthesis methods
- Product Name:2,2-dimethoxyethylsulfanylmethylbenzene
- CAS Number:6304-94-5
- Molecular formula:C11H16O2S
- Molecular Weight:212.31
Yield:6304-94-5 98%
Reaction Conditions:
Stage #1: phenylmethanethiolwith sodium hydride in tetrahydrofuran; for 2 h;Heating;Metallation;
Stage #2: chloroacetaldehyde dimethyl acetal in tetrahydrofuran; for 48 h;Heating;Condensation;
References:
Ong, Chi Wi;Yen, Sin Fei;Chou, Yi Meen [Journal of the Chinese Chemical Society,1999,vol. 46,# 4,p. 601 - 605]
