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ChemicalBook CAS DataBase List 2,2-DiMethyl-2H-1,4-benzoxazin-3(4H)-one, 97%

2,2-DiMethyl-2H-1,4-benzoxazin-3(4H)-one, 97% synthesis

10synthesis methods
-

Yield:10514-70-2 94%

Reaction Conditions:

with 1,8-diazabicyclo[5.4.0]undec-7-ene;1-octyl-3-methylimidazolium tetrafluoroborate at 20; for 2 h;chemoselective reaction;

References:

Sharifi, Ali;Barazandeh, Mehdi;Saeed Abaee;Mirzaei, Mojtaba [Tetrahedron Letters,2010,vol. 51,# 14,p. 1852 - 1855] Location in patent:experimental part