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ChemicalBook CAS DataBase List 2(3H)-Benzothiazolone,7-methyl-(9CI)

2(3H)-Benzothiazolone,7-methyl-(9CI) synthesis

1synthesis methods
201230-82-2 Synthesis
carbon monoxide

201230-82-2
1 suppliers
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3970-40-9 Synthesis
2-CHLORO-3-NITROTOLUENE

3970-40-9
181 suppliers
$8.00/1g

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Yield:80689-19-6 65%

Reaction Conditions:

with water;sulfur;triethylamine in tetrahydrofuran at 80; under 9561.6 Torr; for 10 h;

References:

Konishi, Ken-ichi;Nishiguchi, Ikuzo;Hirashima, Tsuneaki;Sonoda, Noboru;Murai, Shinji [Synthesis,1984,# 3,p. 254 - 255]