ChemicalBook CAS DataBase List 2,5,8,11,14-pentaoxahexadecan-16-oic acid

2,5,8,11,14-pentaoxahexadecan-16-oic acid synthesis

5synthesis methods

Product Name:2,5,8,11,14-pentaoxahexadecan-16-oic acid
CAS Number:16024-66-1
Molecular formula:C11H22O7
Molecular Weight:266.29

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2,5,8,11,14-pentaoxahexadecan-16-oic acid

16024-66-1
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Yield:-

Steps:

Multi-step reaction with 5 steps
1.1: thionyl chloride; triethylamine; dmap / dichloromethane / 0 - 20 °C
2.1: sodium periodate; ruthenium(III) chloride trihydrate / dichloromethane; acetonitrile; water / 0 - 20 °C
3.1: N,N-dimethyl-formamide / 12 h / 20 °C / Inert atmosphere
3.2: 1 h / Inert atmosphere; Reflux
4.1: potassium tert-butylate / tert-butyl alcohol / 2 h / 20 °C
4.2: 12 h / 20 °C
5.1: trifluoroacetic acid; methoxybenzene / dichloromethane / 5 h / 20 °C

References:

Deng, Tao;Mao, Xianglan;Li, Yu;Bo, Shaowei;Yang, Zhigang;Jiang, Zhong-Xing [Bioorganic and Medicinal Chemistry Letters,2018,vol. 28,# 22,p. 3502 - 3505]

23783-42-8 Synthesis