2,6-DIBROMOBENZALDEHYDE synthesis
- Product Name:2,6-DIBROMOBENZALDEHYDE
- CAS Number:67713-23-9
- Molecular formula:C7H4Br2O
- Molecular Weight:263.91
98-11-3
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67713-23-9
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Yield:-
Steps:
Multi-step reaction with 3 steps
1: N-Bromosuccinimide / chloroform / 2.5 h / 40 - 50 °C
2: n-butyllithium; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 1.17 h / -60 - 0 °C
3: phosphoric acid; hydroxyapatite / 1 h / 150 °C / Inert atmosphere
References:
Henan Normal University;Chen Qi;Wang Jiahao;Zhou Yingjie CN109400453, 2019, A
6630-33-7
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67713-23-9
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69321-60-4
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89692-43-3
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55289-36-6
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