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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide

2-Methylene-1,3-dioxane synthesis

1synthesis methods
5695-72-7 Synthesis
2-Chloromethyl-[1,3]dioxane

5695-72-7
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2-Methylene-1,3-dioxane

5663-11-6
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Yield:5663-11-6 89%

Reaction Conditions:

with potassium tert-butylate;Aliquat 336 in tetrahydrofuran at 20;Heating;Dehydrochlorination;

References:

Wu, Zhihong;Stanley, Roy R.;Pittman Jr., Charles U. [Journal of Organic Chemistry,1999,vol. 64,# 22,p. 8386 - 8395]