ChemicalBook CAS DataBase List 10,11-dihydro-5H-Dibenzo[a,d]cycloheptene-5-Methanol

10,11-dihydro-5H-Dibenzo[a,d]cycloheptene-5-Methanol synthesis

6synthesis methods

Product Name:10,11-dihydro-5H-Dibenzo[a,d]cycloheptene-5-Methanol
CAS Number:2975-80-6
Molecular formula:C16H16O
Molecular Weight:224.3

1210-35-1
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$6.00/1g

10,11-dihydro-5H-Dibenzo[a,d]cycloheptene-5-Methanol

2975-80-6
18 suppliers
$45.00/10mg

Yield:-

Steps:

Multi-step reaction with 3 steps
1: 100 percent / sodium bis(trimethylsilyl)amide / dioxane; tetrahydrofuran / 2 h / Heating
2: 81 percent / aq. HClO₄ / diethyl ether / 20 °C
3: 81 percent / NaBH₄ / ethanol / 4 h / 20 °C

References:

Sorensen, Ulrik S;Bleisch, Thomas J;Kingston, Anne E;Wright, Rebecca A;Johnson, Bryan G;Schoepp, Darryle D;Ornstein, Paul L [Bioorganic and medicinal chemistry,2003,vol. 11,# 2,p. 197 - 205]

5H-Dibenzo[a,d]cycloheptene-5-carboxylic acid, 10,11-dihydro-

5018-91-7
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2975-80-6
18 suppliers
$45.00/10mg

References

5H-Dibenzo[a,d]cycloheptene-5-carboxaldehyde, 10,11-dihydro-

24391-61-5
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2975-80-6
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References

5H-Dibenzo[a,d]cycloheptene-5-carboxylic acid, 10,11-dihydro-, methyl ester

16036-72-9
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2975-80-6
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References

Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-

1000210-73-0
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2975-80-6
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References