3,4-DICHLOROBENZYLAMINE HYDROCHLORIDE synthesis
- Product Name:3,4-DICHLOROBENZYLAMINE HYDROCHLORIDE
- CAS Number:49552-34-3
- Molecular formula:C7H8Cl3N
- Molecular Weight:212.5041
6574-99-8
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49552-34-3
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Yield:49552-34-3 83%
Reaction Conditions:
Stage #1: 3,4-dichloro-benzonitrilewith MnBr(CO)2[NH(CH2CH2P(iPr)2)2];hydrogen;sodium t-butanolate in toluene at 120; under 37503.8 Torr; for 24 h;Autoclave;
Stage #2: with hydrogenchloride in diethyl ether;
References:
Elangovan, Saravanakumar;Topf, Christoph;Fischer, Steffen;Jiao, Haijun;Spannenberg, Anke;Baumann, Wolfgang;Ludwig, Ralf;Junge, Kathrin;Beller, Matthias [Journal of the American Chemical Society,2016,vol. 138,# 28,p. 8809 - 8814] Location in patent:supporting information
102-49-8
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49552-34-3
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