3,5-DIIODOSALICYLALDEHYDE synthesis
- Product Name:3,5-DIIODOSALICYLALDEHYDE
- CAS Number:2631-77-8
- Molecular formula:C7H4I2O2
- Molecular Weight:373.91
90-02-8
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$9.00/1g
2631-77-8
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Yield: 87%
Reaction Conditions:
Stage #1:salicylaldehyde with iodine;1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione in dimethyl sulfoxide at 20;
Stage #2: with sodium thiosulfate in water;dimethyl sulfoxide
Stage #3: with ammonium chloride in water
References:
Moorthy, Jarugu Narasimha;Senapati, Kalyan;Kumar, Sarvesh [Journal of Organic Chemistry,2009,vol. 74,# 16,p. 6287 - 6290] Location in patent:supporting information; experimental part
89-95-2
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$22.00/10g
2631-77-8
156 suppliers
$8.00/1g