3-aMino-2-cyanobut-2-enethioaMide synthesis
- Product Name:3-aMino-2-cyanobut-2-enethioaMide
- CAS Number:41808-30-4
- Molecular formula:C5H7N3S
- Molecular Weight:141.19
89943-20-4
8 suppliers
inquiry
41808-30-4
9 suppliers
inquiry
Yield:41808-30-4 80%
Reaction Conditions:
with ammonia in methanol at 20;
Steps:
V-A
A stirred solution of V-2 (30 g, 210 mmol) in a saturated solution of ammonia in methanol (500 mL) was stirred at rt overnight. MeOH was removed under reduced pressure, the aqueous layer was stood overnight, and the precipitate was collected to provide compound V-3 (24 g, yield 80%).
References:
WO2013/25733,2013,A1 Location in patent:Paragraph 0435
5417-82-3
115 suppliers
$9.00/1g
41808-30-4
9 suppliers
inquiry