3-Amino-4-methylisoquinoline synthesis

4synthesis methods

Product Name:3-Amino-4-methylisoquinoline
CAS Number:7697-66-7
Molecular formula:C10H10N2
Molecular Weight:158.2

34824-58-3 Synthesis

34824-58-3
139 suppliers
$9.00/1g

7697-66-7
24 suppliers
inquiry

Yield:-

Steps:

Multi-step reaction with 4 steps
1.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium t-butanolate / 1,4-dioxane / 4 h / 70 °C / Inert atmosphere
2.1: sodium t-butanolate / 1,4-dioxane / 8 h / 70 °C / Inert atmosphere
3.1: ethanol; water / 18 h / 90 °C
4.1: water; ammonium chloride / ethanol / 3 h / 90 °C
4.2: 3 h / 90 °C

References:

Pilgrim, Ben S.;Gatland, Alice E.;McTernan, Charlie T.;Procopiou, Panayiotis A.;Donohoe, Timothy J. [Organic Letters,2013,vol. 15,# 24,p. 6190 - 6193]

Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-

1000210-73-0
0 suppliers
inquiry

7697-66-7
24 suppliers
inquiry

References

6630-33-7
406 suppliers
$9.00/10g

7697-66-7
24 suppliers
inquiry

References

28970-71-0
13 suppliers
inquiry

7697-66-7
24 suppliers
inquiry

References

3-Amino-4-methylisoquinoline Related Search:

5-Bromo-4-methylisoquinoline 4-Amino-1-methylisoquinoline 5-amino-6-methylisoquinoline