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3-Chloro-6-Methylbenzo[b]thiophene-2-carbaldehyde synthesis

2synthesis methods
34576-87-9 Synthesis
3-CHLORO-6-METHYL-BENZO[B]THIOPHENE-2-CARBONYL CHLORIDE

34576-87-9
33 suppliers
$58.00/100mg

3-Chloro-6-Methylbenzo[b]thiophene-2-carbaldehyde

84258-86-6
5 suppliers
inquiry

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Yield:-

Steps:

Multi-step reaction with 2 steps
1: 75 percent / lithium aluminum hydride / diethyl ether / Heating
2: 70 percent / chromium trioxide-pyridine complex / pyridine / Ambient temperature

References:

Tominaga, Yoshinori;Pratap, Ram;Castle, Raymond N.;Lee, Milton L. [Journal of Heterocyclic Chemistry,1982,vol. 19,p. 871 - 877]