3-ISOPROPYLPHENOL synthesis
- Product Name:3-ISOPROPYLPHENOL
- CAS Number:618-45-1
- Molecular formula:C9H12O
- Molecular Weight:136.19
5369-16-4
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618-45-1
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$67.00/5g
Yield:618-45-1 58%
Reaction Conditions:
with uranyl acetate monohydrate;water;trifluoroacetic acid in acetonitrile; for 48 h;Irradiation;Inert atmosphere;
Steps:
4 Example 4
In a 25mL reaction tube, add 3-isopropylaniline (0.2mmol, 27.0mg), water (0.6mmol, 10.8mg), uranyl acetate hydrate (4mol%/0.008mmol, 3.4mg), trifluoroacetic acid ( 0.2mmol, 22.8mg), acetonitrile (2mL), stirred for 2 days under the irradiation of a 6-watt blue LED lamp (wavelength 460nm) in a nitrogen atmosphere. After the reaction is complete, it is extracted, concentrated, and subjected to column chromatography (VPE/VEA=10/ 1) Isolated brown liquid 3d (15.8mg, 58%).
References:
CN112778125,2021,A Location in patent:Paragraph 0050-0053
187737-37-7
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618-45-1
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