ChemicalBook CAS DataBase List 3-(NICOTINOYL-2,4,5,6-D4)-2-PYRROLIDINONE

3-(NICOTINOYL-2,4,5,6-D4)-2-PYRROLIDINONE synthesis

1synthesis methods

Product Name:3-(NICOTINOYL-2,4,5,6-D4)-2-PYRROLIDINONE
CAS Number:764661-25-8
Molecular formula:C10H6D4N2O2
Molecular Weight:194.22

14468-90-7 Synthesis

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3-(NICOTINOYL-2,4,5,6-D4)-2-PYRROLIDINONE

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Yield:-

Reaction Conditions:

Stage #1: N-trimethylsilyl-pyrrolidin-2-onewith n-butyllithium;diisopropylamine in diethyl ether at -78 - -15; for 0.333333 h;
Stage #2: 2,4,5,6-tetradeuterio-nicotinic acid ethyl ester in diethyl ether at -78 - 20;

References:

Gaertner, Peter;Bica, Katharina;Einzinger, Christian [Monatshefte fur Chemie,2004,vol. 135,# 5,p. 549 - 555]