![](/CAS/GIF/10147-11-2.gif)
3-PHENYL-1-PROPYNE synthesis
- Product Name:3-PHENYL-1-PROPYNE
- CAS Number:10147-11-2
- Molecular formula:C9H8
- Molecular Weight:116.16
![trimethyl(3-phenylprop-1-ynyl)silane](/CAS/20180703/GIF/31683-47-3.gif)
31683-47-3
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![3-PHENYL-1-PROPYNE](/CAS/GIF/10147-11-2.gif)
10147-11-2
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$39.00/1g
Yield:10147-11-2 5 g
Reaction Conditions:
with potassium carbonate in methanol at 20; for 2 h;Cooling with ice;
Steps:
21.B Step B: Synthesis of Compound 15
Compound 14 (9.2 g, 48.85 mmol) and 100 ml of methanol were cooled in an ice bath.Add potassium carbonate (33.76 g, 244.2 mmol), stir for 2 h, stir at room temperature overnight.Add ethyl acetate, wash with water, and concentrate to give 5 g of oil.Go directly to the next step.
References:
Shanghai Pharmaceutical Industry Institute;China Pharmaceutical Industry Zongyuan;Zheng Nan;Hao Qun;Zhou Weicheng;Song Chengen;Zhang Peng;He Bo;Cao Yuanchao;Bi Siju CN109776544, 2019, A Location in patent:Paragraph 0321; 0326; 0327
![1-PHENYL-1-PROPYNE](/CAS/GIF/673-32-5.gif)
673-32-5
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![3-PHENYL-1-PROPYNE](/CAS/GIF/10147-11-2.gif)
10147-11-2
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$39.00/1g
![Benzene, (3-bromo-2-propen-1-yl)-](/CAS/GIF/859944-01-7.gif)
859944-01-7
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![3-PHENYL-1-PROPYNE](/CAS/GIF/10147-11-2.gif)
10147-11-2
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$39.00/1g
![1-PHENYL-2-PROPYN-1-OL](/CAS/GIF/4187-87-5.gif)
4187-87-5
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$9.00/1g
![3-PHENYL-1-PROPYNE](/CAS/GIF/10147-11-2.gif)
10147-11-2
64 suppliers
$39.00/1g