1-isopropyl-1H-pyrrole-3-carbaldehyde(SALTDATA: FREE) synthesis
- Product Name:1-isopropyl-1H-pyrrole-3-carbaldehyde(SALTDATA: FREE)
- CAS Number:30186-45-9
- Molecular formula:C8H11NO
- Molecular Weight:137.18
7057-97-8
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23373-77-5
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30186-45-9
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Yield:23373-77-5 14% ，30186-45-9 69%
Reaction Conditions:
Stage #1: diphenylformamidewith trichlorophosphate in 1,1-dichloroethane;Reflux;Vilsmeier-Haack reaction;
Stage #2: N-isopropylpyrrole in 1,1-dichloroethane; for 2 h;Reflux;Vilsmeier-Haack reaction;
Stage #3: with water;sodium acetateregioselective reaction;
References:
Ilyin, Petrv.;Pankova, Alenas.;Kuznetsov, Mikhail A. [Synthesis,2012,vol. 44,# 9,p. 1353 - 1358] Location in patent:experimental part
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23373-77-5
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$63.00/200μmol
30186-45-9
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$45.00/10mg
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2700-30-3
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23373-77-5
17 suppliers
$63.00/200μmol
30186-45-9
22 suppliers
$45.00/10mg
7057-97-8
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52008-97-6
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23373-77-5
17 suppliers
$63.00/200μmol
30186-45-9
22 suppliers
$45.00/10mg
7057-97-8
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54262-97-4
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23373-77-5
17 suppliers
$63.00/200μmol
30186-45-9
22 suppliers
$45.00/10mg