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4,4',6,6'-bipyridine tetracarboxylic acid synthesis

2synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: palladium 10% on activated carbon / 72 h / 160 °C
1.2: 1.5 h / 160 °C
2.1: nitric acid / water / 36 h / 160 °C / High pressure

References:

Li, Ting-Ting;Zhao, Wei-Liang;Chen, Yong;Li, Fu-Min;Wang, Chuan-Jun;Tian, Yong-Hua;Fu, Wen-Fu [Chemistry - A European Journal,2014,vol. 20,# 43,p. 13957 - 13964]