4'-BROMOACETOACETANILIDE synthesis

6synthesis methods

Product Name:4'-BROMOACETOACETANILIDE
CAS Number:95262-09-2
Molecular formula:C9H8BrNO3
Molecular Weight:258.07

Propanoic acid, 3-[(4-bromophenyl)amino]-3-oxo-, methyl ester

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Yield:95262-09-2 103.5 g

Reaction Conditions:

with sodium hydroxide in tetrahydrofuran;methanol at -5 - 10; for 1.33333 h;

References:

Haffner, Curt D.;Becherer, J. David;Boros, Eric E.;Cadilla, Rodolfo;Carpenter, Tiffany;Cowan, David;Deaton, David N.;Guo, Yu;Harrington, Wallace;Henke, Brad R.;Jeune, Michael R.;Kaldor, Istvan;Milliken, Naphtali;Petrov, Kim G.;Preugschat, Frank;Schulte, Christie;Shearer, Barry G.;Shearer, Todd;Smalley, Terrence L.;Stewart, Eugene L.;Stuart, J. Darren;Ulrich, John C. [Journal of Medicinal Chemistry,2015,vol. 58,# 8,p. 3548 - 3571] Location in patent:supporting information