Welcome to chemicalbook!
Chinese English Japanese Germany Korea
400-158-6606
Try our best to find the right business for you.
Do not miss inquiry messages Please log in to view all inquiry messages.

Welcome back!

ChemicalBook CAS DataBase List 4-NITROPICOLINIC ACID

4-NITROPICOLINIC ACID synthesis

5synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: 2 h / 65 - 70 °C
2: 73 percent / H2O / -8 - -7 °C
3: 1.) 90percent H2SO4, 2.) NaNO2 / 1.) 120 deg C, 2 h, 2.) water, 20-25 deg C, 1 h, then 80 deg C, 1 h

References:

Desjardins, Sylvie Y.;Cavell, Kingsley J.;Hoare, Jason L.;Skelton, Brian W.;Sobolev, Alexander N.;White, Allan H.;Keim, Wilhelm [Journal of Organometallic Chemistry,1997,vol. 544,# 2,p. 163 - 174]

4-NITROPICOLINIC ACID Related Search: