(4-(p-tolyloxy)phenyl)methanamine hydrochloride synthesis
- Product Name:(4-(p-tolyloxy)phenyl)methanamine hydrochloride
- CAS Number:262862-66-8
- Molecular formula:C14H16ClNO
- Molecular Weight:249.74
129560-03-8
30 suppliers
$560.00/1g
262862-66-8
58 suppliers
$50.00/10g
Yield:262862-66-8 97%
Reaction Conditions:
with hydrogenchloride in methanol;toluene;Large scale;Reagent/catalyst;
Steps:
5; 8 Example 5
Pass the 4-(4'-methylphenoxy)benzylamine methanol solution obtained in Example 1 through a closed filter to filter out the catalyst to obtain a solution, and the catalyst is applied;The solution was desolventized, toluene was added, hydrochloric acid was added dropwise, a solid was precipitated, and centrifuged,Obtained 55.6 kg of 4-(4'-methylphenoxy)benzylamine hydrochloride,Normalized to 99%, the yield is 97%.
References:
CN113024389,2021,A Location in patent:Paragraph 0033; 0039
106-44-5
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262862-66-8
58 suppliers
$50.00/10g
623-03-0
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$6.00/25g
262862-66-8
58 suppliers
$50.00/10g
37563-42-1
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262862-66-8
58 suppliers
$50.00/10g