ChemicalBook CAS DataBase List 5-Bromo-1-pentene

5-Bromo-1-pentene synthesis

13synthesis methods

Product Name:5-Bromo-1-pentene
CAS Number:1119-51-3
Molecular formula:C5H9Br
Molecular Weight:149.03

1,5-Dibromopentane (100 Kg), N, N-dimethylformamide (100 Kg), and hexamethylphosphoramide (6.2 Kg) were stirred and mixed, and then heated in an oil bath at 140°C for 4 h. Atmospheric distillation collects the fractions, and the collected fractions are washed twice with 100 Kg brine. The organic liquid is distilled to obtain product 5-Bromo-1-pentene.

111-24-0 Synthesis

111-24-0
383 suppliers
$5.00/5g

1119-51-3
350 suppliers
$12.00/5g

Yield:1119-51-3 80.1%

Reaction Conditions:

with N,N,N,N,N,N-hexamethylphosphoric triamide in N,N-dimethyl-formamide at 140; for 4 h;Large scale;Time;Temperature;Reagent/catalyst;

Steps:

1-4 Example 2
1,5-dibromopentane 100KG, N,N-dimethylformamide 100KG, hexamethylphosphoric triamide 6.2KG, stir and mix, then heat in oil bath at 140 for 4h, collect fractions by atmospheric distillation, collect fractions After washing twice with 100KG brine, the upper organic liquid was rectified to obtain 52.0KG, the yield was 80.1%, and the content: 99%.

References:

Pulasi Science And Technology (Shanghai) Co., Ltd.;Lu Dianyun;Li Jing;Cai Weibing CN108046980, 2020, B Location in patent:Paragraph 0021; 0031-0042

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821-09-0 Synthesis

821-09-0
239 suppliers
$21.21/1gm:

1119-51-3
350 suppliers
$12.00/5g

References

3003-84-7
168 suppliers
$52.00/25g

1119-51-3
350 suppliers
$12.00/5g

References

1576-85-8
65 suppliers
$48.70/5g

1119-51-3
350 suppliers
$12.00/5g

References

626-87-9
126 suppliers
$20.00/5g

1119-51-3
350 suppliers
$12.00/5g

References

5-Bromo-1-pentene Related Search:

DL-Limonene 1-Pentene 5-Bromopentan-1-ol TRANS-1,3-PENTADIENE Allyl bromide 1,2-PENTADIENE Cyclopentene 1,2-Dibromocyclopentene 5-BROMO-1-HEXENE 4Z,7Z,10Z,13Z-NONADECATETRAENYL BROMIDE