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ChemicalBook CAS DataBase List 5-carbaMoyl-2-Methoxybenzene-1-sulfonyl chloride

5-carbaMoyl-2-Methoxybenzene-1-sulfonyl chloride synthesis

2synthesis methods
-

Yield:81592-99-6 91%

Reaction Conditions:

Stage #1: 4-methoxyphenylacetamidewith chlorosulfonic acid at 0 - 25; for 12 h;Inert atmosphere;
Stage #2: at 50; for 3 h;Inert atmosphere;

References:

Kornahrens, Anne F.;Cognetta, Armand B.;Brody, Daniel M.;Matthews, Megan L.;Cravatt, Benjamin F.;Boger, Dale L. [Journal of the American Chemical Society,2017,vol. 139,# 20,p. 7052 - 7061] Location in patent:supporting information