5-Fluoroindole synthesis
- Product Name:5-Fluoroindole
- CAS Number:399-52-0
- Molecular formula:C8H6FN
- Molecular Weight:135.14
56341-41-4
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399-52-0
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Yield:399-52-0 92%
Reaction Conditions:
with bis(trimethylsilyl)amide yttrium(III);4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane in toluene at 120; for 36 h;Inert atmosphere;
Steps:
2 Example 3
Under nitrogen protection, 0.5 mmol of raw 5-fluoro-2-indolinone, 1.2 mmol of pinacol borane and catalyst Y [N(SiMe3) 2] 30.05 mmol, 3 mL of toluene, reacted at 120 C for 36 h, and the product isolation yield was 92%.
References:
Wenzhou Medical University;Zhang Junfang;Cai Wenxuan CN110818608, 2020, A Location in patent:Paragraph 0043-0047
32989-58-5
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399-52-0
355 suppliers
$10.00/1g
399-76-8
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399-52-0
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2343-22-8
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399-52-0
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![5-fluoro-1-[(2-nitrophenyl)methyl]-1H-indole](/CAS/GIF/261762-12-3.gif)
261762-12-3
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399-52-0
355 suppliers
$10.00/1g