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5-methyl-3,4-dihydroquinolin-2(1H)-one synthesis

5synthesis methods
201230-82-2 Synthesis
carbon monoxide

201230-82-2
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Benzene, 2-ethenyl-1-methyl-3-nitro-

146667-90-5
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Yield:20151-46-6 73%

Reaction Conditions:

with palladium(II) trifluoroacetate;toluene-4-sulfonic acid in tetrahydrofuran at 80; under 26601.8 Torr; for 20 h;regioselective reaction;

References:

Yang, Li;Shi, Lijun;Xing, Qi;Huang, Kuo-Wei;Xia, Chungu;Li, Fuwei [ACS Catalysis,2018,vol. 8,# 11,p. 10340 - 10348]