6-[(1-methylpiperidin-4-yl)oxy]pyridin-3-amine synthesis
- Product Name:6-[(1-methylpiperidin-4-yl)oxy]pyridin-3-amine
- CAS Number:944401-79-0
- Molecular formula:C11H17N3O
- Molecular Weight:207.27
944401-78-9
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Yield:944401-79-0 860 mg
Reaction Conditions:
with palladium 10% on activated carbon;hydrogen in methanol at 35; under 760.051 Torr;
Steps:
22.2 Step 22.2: 6-(1 -Methylpiperidin-4-yloxy)pyridin-3-ylamine
Step 22.2: 6-(1 -Methylpiperidin-4-yloxy)pyridin-3-ylamine 1.05 g of the compound obtained in step 20.1 are dissolved in 90 ml of MeOH and then hydrogenated at atmospheric pressure at 35°C over 10% Pd/C. The medium is filtered and then evaporated under reduced pressure to give 860 mg of 6-(1 - methylpiperidin-4-yloxy)pyridin-3-ylamine.
References:
WO2013/111106,2013,A1 Location in patent:Page/Page column 109
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