6-Methylbenzo[c]phenanthrene synthesis

6synthesis methods

Product Name:6-Methylbenzo[c]phenanthrene
CAS Number:2381-34-2
Molecular formula:C19H14
Molecular Weight:242.31

13922-41-3 Synthesis

13922-41-3
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2381-34-2
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Yield:-

Steps:

Multi-step reaction with 6 steps
1: palladium diacetate; sodium carbonate / water; N,N-dimethyl-formamide / 20 °C
2: sodium tetrahydroborate / methanol / 0 - 20 °C
3: triphenylphosphine; carbon tetrabromide / acetonitrile / 20 °C
4: potassium carbonate; copper(l) iodide; tetra-(n-butyl)ammonium iodide / acetonitrile / 75 °C
5: potassium carbonate / methanol / 20 °C
6: bis(trifluoromethanesulfonyl)amide; [(C₆F₅)₃PAuNTf₂] / 5 h / 20 °C

References:

Shu, Chao;Li, Long;Chen, Cheng-Bin;Shen, Hong-Cheng;Ye, Long-Wu [Chemistry - An Asian Journal,2014,vol. 9,# 6,p. 1525 - 1529]

Naphthalene, 1-(1-methyl-2-phenylethenyl)-

63269-87-4
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2381-34-2
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References

142598-69-4 Synthesis

142598-69-4
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2381-34-2
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References

93321-14-3
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2381-34-2
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References

154380-65-1
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2381-34-2
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References