Benzene, 1,2-difluoro-4-[(1E)-2-isocyanatoethenyl]- synthesis
- Product Name:Benzene, 1,2-difluoro-4-[(1E)-2-isocyanatoethenyl]-
- CAS Number:936366-62-0
- Molecular formula:C9H5F2NO
- Molecular Weight:181.14
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Yield:-
Reaction Conditions:
in benzene; for 3 h;Heating / reflux;
Steps:
6
Compound 6d (3.4 g, 16.3 mmol) was dissolved in benzene (30 mL) and refluxed for 3 h. The solution was concentrated under reduced pressure at rt and the resulting crude Compound 6e was used without purification in the next reaction.
References:
US2005/176769,2005,A1 Location in patent:Page/Page column 50
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