ASINEX-REAG BAS 03375399 synthesis
- Product Name:ASINEX-REAG BAS 03375399
- CAS Number:38580-22-2
- Molecular formula:C7H8N2O4
- Molecular Weight:184.15
62214-19-1
12 suppliers
$290.00/100mg
38580-22-2
13 suppliers
$166.00/100mg
Yield:38580-22-2 77%
Reaction Conditions:
with water;chloroacetic acid for 24 h;Reflux;
Steps:
2
A 10% aq chloroacetic acid solution (150 ml 159 mmol) was added to 2-(6-methyl-4-oxo-2- thioxo-1 ,2,3,4-tetrahydropyrimidin-5-yl)acetic acid (7.3 g; 36.5 mmol). The mixture was stirred under reflux for 24 h and cooled in an ice-bath. The formed solid was collected by filtration, washed with water and dried under reduced pressure to give 5.17 g (77%) of the title compound as a white solid.
References:
WO2011/15641,2011,A1 Location in patent:Page/Page column 91; 92
626-48-2
374 suppliers
$10.00/25g
64-19-7
1523 suppliers
$10.00/25ML
38580-22-2
13 suppliers
$166.00/100mg
10420-33-4
157 suppliers
$9.00/25g
38580-22-2
13 suppliers
$166.00/100mg