C-(1-PIPERIDIN-1-YL-CYCLOHEXYL)-METHYLAMINE synthesis

6synthesis methods

Product Name:C-(1-PIPERIDIN-1-YL-CYCLOHEXYL)-METHYLAMINE
CAS Number:41805-36-1
Molecular formula:C12H24N2
Molecular Weight:196.33

3867-15-0
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$160.00/0.500g

C-(1-PIPERIDIN-1-YL-CYCLOHEXYL)-METHYLAMINE

41805-36-1
38 suppliers
$45.00/50mg

1-(1-piperidin-1-ylcyclohexyl)methanamine

41805-37-2
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Yield:41805-37-2 74.4%

Reaction Conditions:

with LiAlH₄

Steps:

35 1-(1-Aminomethylcyclohexyl) piperidine

EXAMPLE 35 1-(1-Aminomethylcyclohexyl) piperidine 1-(1-cyanocyclohexyl) piperidine (1.92 g. 0.01 mole) was dissolved in dry ether (50 ml) and added dropwise to a stirred suspension of LiAlH₄ (0.76 g. 0.02 mole) in dry ether (100 ml). The suspension was stirred overnight and worked up as in (1b) to give a colourless oil (1.4 g 74.4%) which on treatment with ethanolic HCl gave colourless needles of 1-(1-aminomethylcyclohexyl) piperidine dihydrochloride m.p. 256°-7°.

References:

US3975443,1976,A

3867-15-0
20 suppliers
$160.00/0.500g

41805-36-1
38 suppliers
$45.00/50mg

References

3867-15-0
20 suppliers
$160.00/0.500g

3319-01-5
58 suppliers
$25.00/5mL

41805-36-1
38 suppliers
$45.00/50mg

References

110-89-4
3 suppliers
$15.96/100ML

41805-36-1
38 suppliers
$45.00/50mg

References

108-94-1 Synthesis

108-94-1
527 suppliers
$12.00/50g

41805-36-1
38 suppliers
$45.00/50mg

References