ethyl 2-(cyclopropylamino)acetate synthesis
- Product Name:ethyl 2-(cyclopropylamino)acetate
- CAS Number:71922-62-8
- Molecular formula:C7H13NO2
- Molecular Weight:143.18
105-36-2
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71922-62-8
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$45.00/10mg
Yield:71922-62-8 100%
Reaction Conditions:
in ethanol; for 1 h;
Steps:
7.A
To a solution of 10 g (0.18 mol) of cyclopropylamine in 50 ml of EtOH was added 7 g (0.04 mol) of ethylbromoacetate and the reaction stirred for 1 h. The reaction was then evaporated to dryness, redissolved in CH2Cl2 washed with water, dried over sodium sulfate and concentrated to afford 6 g (quant.) of the title compound as a colorless oil. MS: 144.1 (MH+).
References:
US2009/12063,2009,A1 Location in patent:Page/Page column 14