ETHYL 5-METHYL-5-HEXENOATE synthesis
- Product Name:ETHYL 5-METHYL-5-HEXENOATE
- CAS Number:39495-82-4
- Molecular formula:C9H16O2
- Molecular Weight:156.22
80352-66-5
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105-53-3
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39495-82-4
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Yield:39495-82-4 57%
Reaction Conditions:
Stage #1: diethyl malonatewith sodium hydride in tetrahydrofuran at 0 - 20;Inert atmosphere;
Stage #2: 4-mesyloxy-2-methylbutene in tetrahydrofuran; for 12 h;Inert atmosphere;Reflux;
Stage #3: with sodium chloride in water;dimethyl sulfoxide at 180 - 200; for 12 h;
References:
Fernández-Mateos;Madrazo, S. Encinas;Teijón, P. Herrero;González, R. Rubio [Journal of Organic Chemistry,2015,vol. 80,# 9,p. 4378 - 4391]
115-11-7
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140-88-5
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39495-82-4
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7425-53-8
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39495-82-4
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3128-06-1
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39495-82-4
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