ChemicalBook CAS DataBase List Imidocarb dipropionate

Imidocarb dipropionate synthesis

3synthesis methods

Product Name:Imidocarb dipropionate
CAS Number:55750-06-6
Molecular formula:C22H26N6O3
Molecular Weight:422.49

Midoca dipropionate is a new type of animal-specific antiprotozoal chemical drug for the treatment and prevention of various babesiosis, piriformis, trypanosomes, eperythrocytes, anaplasma borderline and Theileria various diseases caused. It can be synthesized by the reaction of imidazolide and ethyl acetate.

802294-64-0 Synthesis

802294-64-0
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27885-92-3
152 suppliers
$29.00/5mg

55750-06-6
331 suppliers
$10.00/250mg

Yield:55750-06-6 110.8 g

Reaction Conditions:

in ethyl acetate for 0.5 h;

Steps:

10 Synthesis of compound 1
Sequentially add the crude imidazolide (85g, 0.24mol) and 340mL ethyl acetate into a 1L three-necked flask,Heat and stir to reflux, the solids are all dissolved, add 4.3g activated carbon, reflux and stir for 0.5h,Filter, stir the filtrate to room temperature, add propionic acid (39.2g, 0.53mol) dropwise, after about 0.5h, a large amount of white solid precipitates out, cool to 510, stir and crystallize for 2h,Filter, wash the filter cake with a small amount of ethyl acetate, and dry the product under vacuum to obtain white solid imidazolide dipropionate (110.8 g, 93percent).

References:

Shandong Pharmacy Academy Of Sciences;Kong Xiangyu;Yang Li;Cui Xinqiang;Fan Zhiping;Zhang Bin;Li Xinzhi;Liu Wentao;Duan Chonggang;Cui Yan;Ren Yeming CN111574455, 2020, A Location in patent:Paragraph 0013; 0057-0059

619-24-9 Synthesis

619-24-9
259 suppliers
$10.00/1g

55750-06-6
331 suppliers
$10.00/250mg

References

4,5-dihydro-2-(3-nitrophenyl)-1H-imidazole

31659-42-4
15 suppliers
inquiry

55750-06-6
331 suppliers
$10.00/250mg

References

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