N-(Trifluoroacetyl)-L-Ala-L-Phe-OMe synthesis
2synthesis methods
- Product Name:N-(Trifluoroacetyl)-L-Ala-L-Phe-OMe
- CAS Number:329-36-2
- Molecular formula:C15H17F3N2O4
- Molecular Weight:346.3
Yield:329-36-2 94%
Reaction Conditions:
with 2,4-bis(trifluoromethyl)phenylboronic acid in 1,2-dichloro-ethane at 60; for 48 h;Molecular sieve;diastereoselective reaction;
References:
Wang, Ke;Lu, Yanhui;Ishihara, Kazuaki [Chemical Communications,2018,vol. 54,# 43,p. 5410 - 5413] Location in patent:supporting information
