ChemicalBook CAS DataBase List naphthalene-1,3,6,8-tetrol

naphthalene-1,3,6,8-tetrol synthesis

13synthesis methods

Product Name:naphthalene-1,3,6,8-tetrol
CAS Number:18512-30-6
Molecular formula:C10H8O4
Molecular Weight:192.17

58605-10-0 Synthesis

58605-10-0
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18512-30-6
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Yield:-

Steps:

Multi-step reaction with 8 steps
1: 98 percent / LiAlH₄ / diethyl ether
2: 84 percent / NEt₃ / CH₂Cl₂
3: 69 percent / BzNEt₃Cl / CHCl₃; H₂O
4: 92 percent / Ba(OH)2 / dioxane; H₂O
5: diethyl ether
6: 99 percent / 60percent HClO₄ / H₂O; acetic acid
7: 97 percent / H₂ / Pd/C (5percent) / ethyl acetate; ethanol
8: CH₃ONa / methanol

References:

Ichinose, Koji;Ebizuka, Yutaka;Sankawa, Ushio [Chemical and pharmaceutical bulletin,1989,vol. 37,# 10,p. 2873 - 2875]

129-96-4
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18512-30-6
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References

64954-45-6
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18512-30-6
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References

Benzeneacetic acid, 3,5-bis(phenylmethoxy)-, methyl ester

79762-35-9
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18512-30-6
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References

Benzeneacetic acid, 2-acetyl-3,5-bis(phenylmethoxy)-, methyl ester

65857-78-5
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18512-30-6
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References