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TERT-BUTYL 4-(BROMOMETHYL)PHENYL(METHYL)CARBAMATE synthesis

6synthesis methods
-

Yield:168830-93-1 43%

Reaction Conditions:

with carbon tetrabromide;triphenylphosphine in dichloromethane at 0; for 1 h;

References:

Gillespie, Roger J.;Bamford, Samantha J.;Botting, Ruth;Comer, Mike;Denny, Sarah;Gaur, Suneel;Griffin, Michael;Jordan, Allan M.;Knight, Anthony R.;Lerpiniere, Joanne;Leonardi, Stefania;Lightowler, Sean;McAteer, Steven;Merrett, Angela;Misra, Anil;Padfield, Antony;Reece, Mark;Saadi, Mona;Selwood, Daniel L.;Stratton, Gemma C.;Surry, Dominic;Todd, Richard;Tong, Xin;Ruston, Vicki;Upton, Rebecca;Weiss, Scott M. [Journal of Medicinal Chemistry,2009,vol. 52,# 1,p. 33 - 47] Location in patent:experimental part