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Z-VAL-NHTBU synthesis

3synthesis methods
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Yield:61274-17-7 82%

Reaction Conditions:

with 4-methyl-morpholine;1-hydroxy-7-aza-benzotriazole;1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride in dichloromethane; for 16 h;Inert atmosphere;

References:

Le Bailly, Bryden A. F.;Clayden, Jonathan [Chemical Communications,2014,vol. 50,# 59,p. 7949 - 7952] Location in patent:supporting information