| Identification | Back Directory | [Name]
1-broMo-2-chloro-4-fluoro-5-nitrobenzene | [CAS]
111010-08-3 | [Synonyms]
YVDJBLFLBBBGMD-UHFFFAOYSA-N
5-bromo-4-chloro-2-fluoronitrobenzene
1-broMo-2-chloro-4-fluoro-5-nitrobenzene
Benzene, 1-bromo-2-chloro-4-fluoro-5-nitro- | [Molecular Formula]
C6H2BrClFNO2 | [MDL Number]
MFCD20528320 | [MOL File]
111010-08-3.mol | [Molecular Weight]
254.44 |
| Chemical Properties | Back Directory | [Melting point ]
65-65.5 °C | [Boiling point ]
290.0±35.0 °C(Predicted) | [density ]
1.904±0.06 g/cm3(Predicted) | [storage temp. ]
Sealed in dry,Room Temperature | [form ]
powder | [color ]
Faint to light yellow |
| Hazard Information | Back Directory | [Synthesis]
To a mixture of 4-chloro-2-fluoronitrobenzene (1.00 g), silver sulfate (1.95 g), and concentrated sulfuric acid (5 ml), bromine (0.32 ml) was added under ice cooling, and the resulting mixture was stirred at 0 C. for 30 min, then at room temperature for 1 h. The reaction mixture was put into ice water and subjected to extraction with ether. The organic layer was washed with water, a saturated aqueous sodium hydrogen carbonate solution, and a saturated aqueous sodium chloride solution sequentially, dried with anhydrous sodium sulfate and concentrated under reduced pressure to give 1.38 g of 1-Bromo-2-chloro-4-fluoro-5-nitrobenzene (yield, 95%).
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