ChemicalBook--->CAS DataBase List--->112581-77-8

112581-77-8

112581-77-8 Structure

112581-77-8 Structure
IdentificationBack Directory
[Name]

2,6-DICHLOROIMIDAZO[1,2-B]PYRIDAZINE
[CAS]

112581-77-8
[Synonyms]

2,6-DICHLOROIMIDAZO[1,2-B]PYRIDAZINE
IMidazo[1,2-b]pyridazine,2,6-dichloro-
2,6-DICHLOROIMIDAZO[1,2-B]PYRIDAZINE ISO 9001:2015 REACH
[Molecular Formula]

C6H3Cl2N3
[MDL Number]

MFCD11044765
[MOL File]

112581-77-8.mol
[Molecular Weight]

188.01
Chemical PropertiesBack Directory
[density ]

1.69
[storage temp. ]

2-8°C
[InChI]

InChI=1S/C6H3Cl2N3/c7-4-1-2-6-9-5(8)3-11(6)10-4/h1-3H
[InChIKey]

MGNCSIAIZSTMHX-UHFFFAOYSA-N
[SMILES]

C12=NC(Cl)=CN1N=C(Cl)C=C2
Safety DataBack Directory
[Symbol(GHS) ]

Exclamation Mark (GHS07)
GHS07
[Signal word ]

Warning
[Hazard statements ]

H302-H315-H319-H332-H335
[Precautionary statements ]

P261-P280-P305+P351+P338
[HS Code ]

2933998090
Hazard InformationBack Directory
[Synthesis]

6-Chloro-3-imino-2,3-dihydropyridazine-2-acetic acid

127566-18-1

2,6-DICHLOROIMIDAZO[1,2-B]PYRIDAZINE

112581-77-8

Example 4: 1.88 g of 6-chloro-3-imino-2,3-dihydropyridazine-2-acetic acid (purity: 99.5 wt%) was mixed with 7.52 g of monochlorobenzene and 0.79 g of pyridine. 3.84 g of phosphoryl chloride was slowly added dropwise to the mixture over a period of 3 minutes at an endothermic condition of 20 to 40 °C. Subsequently, the reaction system was heated to an endothermic temperature of 120 °C within 20 minutes and the reaction was continued at this temperature for 6 hours. Upon completion of the reaction, the mixture was cooled to give a reaction mixture containing 2,6-dichloroimidazo[1,2-b]pyridazine.The yield of 2,6-dichloroimidazo[1,2-b]pyridazine was 99%.

[References]

[1] Patent: EP1930331, 2008, A1. Location in patent: Page/Page column 5
[2] Patent: EP1930331, 2008, A1. Location in patent: Page/Page column 4
[3] Patent: EP1930331, 2008, A1. Location in patent: Page/Page column 4
[4] Patent: EP1930331, 2008, A1. Location in patent: Page/Page column 5
[5] Patent: EP1930331, 2008, A1. Location in patent: Page/Page column 5
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