| Identification | Back Directory | [Name]
4-Methyloxindole | [CAS]
13220-46-7 | [Synonyms]
13220-46-7
4-Methyloxindole
4-Methyl-2-oxindole
4-Methyloxindole,95%
4-methylindolin-2-one
4-Methyl-1,3-dihydro-indol-2-one
4-methyl-2-oxo-1,2-dihydro-indole
1,3-dihydro-4-methyl-2H-Indol-2-one
2H-Indol-2-one, 1,3-dihydro-4-methyl-
4-methyl-1,3-dihydroindol-2-one in stock Factory | [Molecular Formula]
C9H9NO | [MDL Number]
MFCD09835631 | [MOL File]
13220-46-7.mol | [Molecular Weight]
147.174 |
| Chemical Properties | Back Directory | [Melting point ]
211 °C | [Boiling point ]
318.4±41.0 °C(Predicted) | [density ]
1.155±0.06 g/cm3(Predicted) | [storage temp. ]
Sealed in dry,Room Temperature | [form ]
Solid | [pka]
14.21±0.20(Predicted) | [Appearance]
White to yellow Solid |
| Hazard Information | Back Directory | [Synthesis]
General procedure for the synthesis of 4-methylindolone from 2-(2-methyl-6-nitrophenyl)acetic acid: 2-(2-methyl-6-nitrophenyl)acetic acid (1.4 g, 7 mmol) was dissolved in 20 mL of methanol, 0.14 g of 10% palladium/carbon catalyst was added, and the reaction was placed in a Parr oscillator and hydrogenated for 3 hours at 60 psi hydrogen pressure. Upon completion of the reaction, the catalyst was removed by filtration followed by evaporation to remove the solvent. The brown solid obtained was ground with ethyl acetate and dried under vacuum to yield 0.9 g (74% yield) of 4-methylindolone as a white solid. | [References]
[1] Patent: US2004/186160, 2004, A1. Location in patent: Page/Page column 22
[2] Patent: US6878733, 2005, B1. Location in patent: Page/Page column 168; 217
[3] Patent: US6350754, 2002, B2. Location in patent: Page column 19-20 |
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| Company Name: |
Energy Chemical
|
| Telephone: |
400-0056266 |
| Website: |
www.energy-chemical.com |
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