| Identification | Back Directory | [Name]
4-c]pyridine | [CAS]
1357947-08-0 | [Synonyms]
5-broMo-3-iodo-1H-pyrazolo[3,4-c]pyridine
1H-Pyrazolo[3,4-c]pyridine, 5-bromo-3-iodo- | [Molecular Formula]
C6H3BrIN3 | [MDL Number]
MFCD21647868 | [MOL File]
1357947-08-0.mol | [Molecular Weight]
323.917 |
| Chemical Properties | Back Directory | [Boiling point ]
458.7±40.0 °C(Predicted) | [density ]
2.559±0.06 g/cm3(Predicted) | [storage temp. ]
under inert gas (nitrogen or Argon) at 2–8 °C | [form ]
solid | [pka]
7.72±0.40(Predicted) | [Appearance]
Off-white to light yellow Solid |
| Hazard Information | Back Directory | [Synthesis]
Step I. Preparation of 5-bromo-1H-pyrazolo[3,4-c]pyridine
To a solution of 6-bromo-4-methylpyridin-3-amine (7.76 g, 0.0415 mol) in acetic acid (412.8 mL, 7.260 mol) was added 4.0 ml of a 4.0 ml aqueous solution of sodium nitrite (2.87 g, 0.041 |
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