| Identification | Back Directory | [Name]
2,3 DIBROMO-5-CHLORO PYRIDINE | [CAS]
137628-17-2 | [Synonyms]
2,3-Dibromo-5-chL
7-Bromopicolinic acid
3-Dibromo-5-chloropyridine
5-CHLORO-2,3-DIBROMOPYRIDINE
2,3 DIBROMO-5-CHLORO PYRIDINE
2,3-DIBROMO-5-DICHLOROPYRIDINE
Pyridine, 2,3-dibromo-5-chloro-
2,3-Dibromo-5-chloropyridine>
2,3-Dibromo-5-chloropyridine 98%
2,3-DibroMo-5-chloropyridine, 97+%
Pyridine2,3-dibromo-5-chloropyridine
2,3 DIBROMO-5-CHLORO PYRIDINE ISO 9001：2015 REACH | [Molecular Formula]
C5H2Br2ClN | [MDL Number]
MFCD08687254 | [MOL File]
137628-17-2.mol | [Molecular Weight]
271.337 |
| Chemical Properties | Back Directory | [Melting point ]
41.0 to 45.0 °C | [Boiling point ]
259.9±35.0 °C(Predicted) | [density ]
2.136±0.06 g/cm3(Predicted) | [storage temp. ]
Inert atmosphere,Room Temperature | [solubility ]
soluble in Methanol | [form ]
powder to crystal | [pka]
-3.85±0.20(Predicted) | [color ]
White to Light yellow to Light orange | [InChI]
InChI=1S/C5H2Br2ClN/c6-4-1-3(8)2-9-5(4)7/h1-2H | [InChIKey]
GDUFWKJMOOVEMX-UHFFFAOYSA-N | [SMILES]
C1(Br)=NC=C(Cl)C=C1Br |
| Hazard Information | Back Directory | [Uses]
2,3-Dibromo-5-chloropyridine has been used as a reactant for regiospecific Grignard reactions with lactones. | [Synthesis]
3-Bromo-5-chloropyridone (8.0 g, 38.4 mmole) was dissolved in dimethylformamide (60 ml) at ambient temperature. Phosphorus (V) tribromide oxide (16.5 g, 57.6 mmoles) was added and the reaction heated to 80° C for 72 hours. After cooling, the reaction was poured onto 800 g of ice. Vacuum filtration provided the product as a dark solid (6.85 g). Hexane (225 ml) and decolorizing carbon was added to the crude product and the contents heated to reflux and then filtered through celite. The clear colorless filtrate was stripped under vacuum to yield 2,3-Dibromo-5-chloropyridine as a white solid (5.3 g, 51%).
 | [References]
[1] Patent: US5436344, 1995, A |
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J & K SCIENTIFIC LTD.
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18210857532 18210857532 |
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https://www.jkchemical.com |
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Alfa Aesar
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400-6106006 |
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Jia Xing Isenchem Co.,Ltd
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